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X-ray powder diffraction camera

X-ray powder diffraction camera

Date: circa 1955
Inventory Number: 2004-1-0321
Classification: X-Ray Diffraction Camera
Subject:
geology, mineralogy, crystallography, spectroscopy,
User: Mineralogical Museum, Harvard University (founded circa 1775)
Cultural Region:
United States,
City of Use:
Cambridge,
Dimensions:
18 × 16.2 × 9 cm (7 1/16 × 6 3/8 × 3 9/16 in.)
Material:
wax, brass, steel, iron,
Description:
Upright circular chamber fixed on a solid base that can be mounted on a slider. The cylindrical part has two diametrically opposed orifices in which there are screwed two pinhole collimators. The top of the cylinder has a detachable round lid. In the center of the cylinder there is a pin where the specimen is to be mounted. On top there are two screws, one used to fix the X-ray film, and the second to center the sample holder.

Signedunsigned
Inscribedlabel: MIN 104;

label: RETURN TO BERMAN LAB;

label: 5
FunctionAn X-ray diffraction camera can be used to determine the atomic arrangement of crystals.

The wavelength of an X-ray is similar in size to the distance between atoms in crystalline substances. Thus, by recording how a material scatters X-rays, and causes variation in their intensity, one may determine its crystal structure - the pattern by which its atoms are arranged as well as the precise distance between them.

This powder X-ray camera (also known as a Debye-Scherrer camera) consists of a light-tight cylindrical enclosure which holds a strip of X-ray film accurately fixed on its perimeter. The specimen, usually a fine powder, is accurately placed on the axis of the cylinder. A fine beam of X-rays, produced by passing the beam through a metal collimator, is scattered on the sample. The pattern of lines on the photograph represents possible values of the Bragg angles that satisfy Bragg’s law .
Curatorial RemarksFor a similar model see 2004-1-0320.
ProvenanceCarl Francis, Mineralogical Museum, Harvard University
Related WorksA useful introduction to X-ray powder diffraction methods can be found here . Also, see M.M. Woolfson, An introduction to X-ray crystallography ( Cambridge University Press, 1997), p. 112-8

For more pictures of Debye-Scherrer cameras see this website

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